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ISO 9388:1992

Nickel alloys - Determination of phosphorus content - Molybdenum blue molecular absorption spectrometric method
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ISO 9388:1992

Nickel alloys - Determination of phosphorus content - Molybdenum blue molecular absorption spectrometric method

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Phosphorus content can be determined in the range of 0,001 % (m/m) to 0,025 % (m/m). Cr(III) and silica cause interference which is eliminated. The principle is dissolution of a test portion in a mixture of nitric and hydrochloric acids, fuming with sulfuric acid, oxidation of Cr(III) to Cr(VI), precipitation of Fe(III) phosphate and redissolution of the precipitate, addition of boric, tartaric and sulfamic acids, formation and extraction of molybdophosphoric acid, reduction of the heteropoly acid to molybdenum blue and back-extraction into an aqueous phase, measurement of the absorbance of the aqueous solution at 700 nm.

SDO ISO: International Organization for Standardization
Document Number ISO 9388
Publication Date Not Available
Language en - English
Page Count
Revision Level
Supercedes
Committee ISO TC 155/SC 3
Publish Date Document Id Type View
Not Available ISO 9388:1992 Revision